EPA方法16145
Mixtures of PBDEs Standard Solution for Accuracy & Precision
BDE-AAP-A $ 195 / 1 x 1 mL
At stated conc. in Isooctane 39 comps.
ng/mL
2-Bromodiphenyl ether (#1) 100
3-Bromodiphenyl ether (#2) 100
4-Bromodiphenyl ether (#3) 100
2,4-Dibromodiphenyl ether (#7) 100
2,4'-Dibromodiphenyl ether (#8) 100
2,6-Dibromodiphenyl ether (#10) 100
3,3'-Dibromodiphenyl ether (#11) 100
3,4-Dibromodiphenyl ether (#12) 100
3,4'-Dibromodiphenyl ether (#13) 100
4,4'-Dibromodiphenyl ether (#15) 100
2,2',4,-Tribromodiphenyl ether (#17) 100
2,3',4-Tribromodiphenyl ether (#25) 100
2,4,4'-Tribromodiphenyl ether (#28) 100
2,4,6-Tribromodiphenyl ether (#30) 100
2,4',6-Tribromodiphenyl ether (#32) 100
2',3,4-Tribromodiphenyl ether (#33) 100
3,3',4-Tribromodiphenyl ether (#35) 100
3,4,4'-Tribromodiphenyl ether (#37) 100
2,2',4,4'-Tetrabromodiphenyl ether (#47) 100
2,2',4,5'-Tetrabromodiphenyl ether (#49) 100
2,3',4,4'-Tetrabromodiphenyl ether (#66) 100
2,3',4',6-Tetrabromodiphenyl ether (#71) 100
2,4,4',6-Tetrabromodiphenyl ether (#75) 100
3,3',4,4'-Tetrabromodiphenyl ether (#77) 100
2,2',3,4,4'-Pentabromodiphenyl ether (#85) 150
2,2',4,4',5-Pentabromodiphenyl ether (#99) 150
2,2',4,4',6-Pentabromodiphenyl ether (#100) 150
2,3,4,5,6-Pentabromodiphenyl ether (#116) 150
2,3',4,4',5-Pentabromodiphenyl ether (#118) 150
2,3',4,4',6-Pentabromodiphenyl ether (#119) 150
3,3',4,4',5-Pentabromodiphenyl ether (#126) 150
2,2',3,4,4',5'-Hexabromodiphenyl ether (#138) 200
2,2',4,4',5,5'-Hexabromodiphenyl ether (#153) 200
2,2',4,4',5,6'-Hexabromodiphenyl ether (#154) 200
2,2',4,4',6,6'-Hexabromodiphenyl ether (#155) 200
2,3,4,4',5,6-Hexabromodiphenyl ether (#166) 200
2,2',3,4,4',5,6-Heptabromodiphenyl ether (#181) 250
2,2',3,4,4',5',6-Heptabromodiphenyl ether (#183) 250
2,3,3',4,4',5,6-Heptabromodiphenyl ether (#190) 250
BDE-AAP-A-15X $ 750 / 1 x 1 mL
At stated conc. in Isooctane 39 comps.
μg/mL
2-Bromodiphenyl ether (#1) 1.5
3-Bromodiphenyl ether (#2) 1.5
4-Bromodiphenyl ether (#3) 1.5
2,4-Dibromodiphenyl ether (#7) 1.5
2,4'-Dibromodiphenyl ether (#8) 1.5
2,6-Dibromodiphenyl ether (#10) 1.5
3,3'-Dibromodiphenyl ether (#11) 1.5
3,4-Dibromodiphenyl ether (#12) 1.5
3,4'-Dibromodiphenyl ether (#13) 1.5
4,4'-Dibromodiphenyl ether (#15) 1.5
2,2',4-Tribromodiphenyl ether (#17) 1.5
2,3',4-Tribromodiphenyl ether (#25) 1.5
2,4,4'-Tribromodiphenyl ether (#28) 1.5
2,4,6-Tribromodiphenyl ether (#30) 1.5
2,4',6-Tribromodiphenyl ether (#32) 1.5
2',3,4-Tribromodiphenyl ether (#33) 1.5
3,3',4-Tribromodiphenyl ether (#35) 1.5
3,4,4'-Tribromodiphenyl ether (#37) 1.5
2,2',4,4'-Tetrabromodiphenyl ether (#47) 1.5
2,2',4,5'-Tetrabromodiphenyl ether (#49) 1.5
2,3',4,4'-Tetrabromodiphenyl ether (#66) 1.5
2,3',4',6-Tetrabromodiphenyl ether (#71) 1.5
2,4,4',6-Tetrabromodiphenyl ether (#75) 1.5
3,3',4,4'-Tetrabromodiphenyl ether (#77) 1.5
2,2',3,4,4'-Pentabromodiphenyl ether (#85) 2.25
2,2',4,4',5-Pentabromodiphenyl ether (#99) 2.25
2,2',4,4',6-Pentabromodiphenyl ether (#100) 2.25
2,3,4,5,6-Pentabromodiphenyl ether (#116) 2.25
2,3',4,4',5-Pentabromodiphenyl ether (#118) 2.25
2,3',4,4',6-Pentabromodiphenyl ether (#119) 2.25
3,3',4,4',5-Pentabromodiphenyl ether (#126) 2.25
2,2',3,4,4',5'-Hexabromodiphenyl ether (#138) 3.0
2,2',4,4',5,5'-Hexabromodiphenyl ether (#153) 3.0
2,2',4,4',5,6'-Hexabromodiphenyl ether (#154) 3.0
2,2',4,4',6,6'-Hexabromodiphenyl ether (#155) 3.0
2,3,4,4',5,6-Hexabromodiphenyl ether (#166) 3.0
2,2',3,4,4',5,6-Heptabromodiphenyl ether (#181) 3.75
2,2',3,4,4',5',6-Heptabromodiphenyl ether (#183) 3.75
2,3,3',4,4',5,6-Heptabromodiphenyl ether (#190) 3.75
Mixture of Commonly Occurring PBDE
Congeners for Precision and Recovery
BDE-COC $ 600 / 1 x 1 mL
At stated conc. in Isooctane 14 comps.
μg/mL
2,2',4,-Tribromodiphenyl ether (#17) 5
2,4,4'-Tribromodiphenyl ether (#28) 5
2,2',4,4'-Tetrabromodiphenyl ether (#47) 5
2,3',4,4'-Tetrabromodiphenyl ether (#66) 5
2,3',4',6-Tetrabromodiphenyl ether (#71) 5
2,2',3,4,4'-Pentabromodiphenyl ether (#85) 5
2,2',4,4',5-Pentabromodiphenyl ether (#99) 5
2,2',4,4',6-Pentabromodiphenyl ether (#100) 5
2,2',3,4,4',5'-Hexabromodiphenyl ether (#138) 5
2,2',4,4',5,5'-Hexabromodiphenyl ether (#153) 5
2,2',4,4',5,6'-Hexabromodiphenyl ether (#154) 5
2,2',3,4,4',5',6-Heptabromodiphenyl ether (#183) 5
2,3,3',4,4',5,6-Heptabromodiphenyl ether (#190) 5
Decabromodiphenyl ether (#209) 25
PBDE Congeners of Primary Interest
BDE-CSM $ 225 / 1 x 1 mL
At stated conc. in Isooctane 8 comps.
μg/mL
2,4,4'-Tribromodiphenyl ether (#28) 20
2,2',4,4'-Tetrabromodiphenyl ether (#47) 20
2,2',4,4',5-Pentabromodiphenyl ether (#99) 20
2,2',4,4',6-Pentabromodiphenyl ether (#100) 20
2,2',4,4',5,5'-Hexabromodiphenyl ether (#153) 20
2,2',4,4',5,6'-Hexabromodiphenyl ether (#154) 20
2,2',3,4,4',5',6-Heptabromodiphenyl ether (#183) 20
Decabromodiphenyl ether (#209) 200
Calibration Mix
BDE-CM $ 65 / 1 x 1 mL
At stated conc. in Isooctane 8 comps.
μg/mL
2,4,4'-Tribromodiphenyl ether (#28) 2.5
2,2',4,4'-Tetrabromodiphenyl ether (#47) 2.5
2,2',4,4',5-Pentabromodiphenyl ether (#99) 2.5
2,2',4,4',6-Pentabromodiphenyl ether (#100) 2.5
2,2',4,4',5,5'-Hexabromodiphenyl ether (#153) 2.5
2,2',4,4',5,6'-Hexabromodiphenyl ether (#154) 2.5
2,2',3,4,4',5',6-Heptabromodiphenyl ether (#183) 2.5
Decabromodiphenyl ether (#209) 25
Matrix Spiking Solution
BDE-MS $ 40 / 1 x 1 mL
At stated conc. in Isooctane 8 comps.
ng/mL
2,4,4'-Tribromodiphenyl ether (#28) 1
2,2',4,4'-Tetrabromodiphenyl ether (#47) 1
2,2',4,4',5-Pentabromodiphenyl ether (#99) 1
2,2',4,4',6-Pentabromodiphenyl ether (#100) 1
2,2',4,4',5,5'-Hexabromodiphenyl ether (#153) 1
2,2',4,4',5,6'-Hexabromodiphenyl ether (#154) 1
2,2',3,4,4',5',6-Heptabromodiphenyl ether (#183) 1
Decabromodiphenyl ether (#209) 10
PBDEs in Method 1614 Set
BDE-EPA-SET $ 500 / 8 x 1 mL
50 μg/mL each in Isooctane 8 comps.
2,4,4'-Tribromodiphenyl ether (#28)
2,2',4,4'-Tetrabromodiphenyl ether (#47)
2,2',4,4',5-Pentabromodiphenyl ether (#99)
2,2',4,4',6-Pentabromodiphenyl ether (#100)
2,2',4,4',5,5'-Hexabromodiphenyl ether (#153)
2,2',4,4',5,6'-Hexabromodiphenyl ether (#154)
2,2',3,4,4',5',6-Heptabromodiphenyl ether(#183)
Decabromodiphenyl ether (#209)